The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 27, 2022

Filed:

Jan. 25, 2021
Applicant:

Ut-battelle, Llc, Oak Ridge, TN (US);

Inventors:

Luc L. Daemen, Oak Ridge, TN (US);

Robert L. Sacci, Oak Ridge, TN (US);

Beth L. Armstrong, Oak Ridge, TN (US);

Nathan Kidder, Oak Ridge, TN (US);

Assignee:

UT-BATTELLE, LLC, Oak Ridge, TN (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
H01B 1/08 (2006.01); H01M 10/05 (2010.01); C01G 25/02 (2006.01); H01M 10/0562 (2010.01);
U.S. Cl.
CPC ...
C01G 25/02 (2013.01); H01B 1/08 (2013.01); H01M 10/0562 (2013.01); C01P 2006/40 (2013.01); H01M 2300/0068 (2013.01);
Abstract

A method of preparing a lithium-ion conducting garnet via low-temperature solid-state synthesis is disclosed. The lithium-ion conducting garnet comprises a substantially phase pure aluminum-doped cubic lithium lanthanum zirconate (LiLaZrO). The method includes preparing nanoparticles comprising lanthanum zirconate (LaZrO-np) via pyrolysis-mediated reaction of lanthanum nitrate (La(NO)) and zirconium nitrate (Zr(NO)). The method also includes pyrolyzing a solid-state mixture comprising the LaZrO-np, lithium nitrate (LiNO), and aluminum nitrate (Al(NO)) to give the LiLaZrOand thereby prepare the lithium-ion conducting garnet. A lithium-ion conducting garnet prepared via the method is also disclosed.


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