The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 06, 2022

Filed:

Feb. 11, 2019
Applicant:

Basf SE, Ludwigshafen am Rhein, DE;

Inventors:

Oliver Bussmann, Ludwigshafen am Rhein, DE;

Eva Koch, Ludwigshafen am Rhein, DE;

Manfred Heilig, Ludwigshafen am Rhein, DE;

Joachim Pfeffinger, Ludwigshafen am Rhein, DE;

Joerg Pastre, Ludwigshafen am Rhein, DE;

Johann-Peter Melder, Ludwigshafen am Rhein, DE;

Assignee:

BASF SE, Ludwigshafen am Rhein, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 217/08 (2006.01); C07C 41/42 (2006.01); C07C 213/02 (2006.01); C07C 213/10 (2006.01); C07D 295/03 (2006.01); C07D 295/023 (2006.01);
U.S. Cl.
CPC ...
C07D 295/023 (2013.01); C07C 41/42 (2013.01);
Abstract

A process for the continuous distillative separation of mixtures comprising morpholine (MO), monoaminodiglycol (ADG), ammonia, water and methoxyethanol (MOE), obtained by reacting diethylene glycol (DEG) with ammonia, wherein ammonia, water, ADG and DEG are removed by distillation and the resulting stream comprising MO and MOE is supplied to a distillation column Kin which at a top pressure of from 20 to 2000 mbar MO, MOE and organic products having a boiling point 128° C. (1.013 bar) are removed via the bottom and organic products having a boiling point 128° C. are removed overhead, and also MO is removed via a side draw, where Kis equipped with an evaporator for heating the bottoms, into which is fed heating vapor having a pressure of from 1 to 10 bar.


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