The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 01, 2022

Filed:

Nov. 10, 2020
Applicants:

National Technology & Engineering Solutions of Sandia, Llc, Albuquerque, NM (US);

Unm Rainforest Innovations, Albuquerque, NM (US);

Inventors:

Stephen Percival, Albuquerque, NM (US);

James Eujin Park, Albuquerque, NM (US);

Ivana Gonzales, Santa Fe, NM (US);

Stanley Shihyao Chou, Albuquerque, NM (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 27/051 (2006.01); B01J 35/00 (2006.01); B01J 37/16 (2006.01); B01J 37/08 (2006.01); B82Y 40/00 (2011.01); B82Y 30/00 (2011.01);
U.S. Cl.
CPC ...
B01J 27/0515 (2013.01); B01J 35/006 (2013.01); B01J 35/0033 (2013.01); B01J 37/08 (2013.01); B01J 37/16 (2013.01); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01);
Abstract

An electrocatalyst comprises a crumpled transition metal dichalcogenide support loaded with catalytic metal nanoparticles through spontaneous reduction reactions. The support can be prepared by hydrothermal conversion of 2D nanosheets to 3D hierarchically crumpled sheets. As an example, using crumpled MoSas a support, highly tunable Ru loadings were obtained using the electrostatic interaction between MoSand RuClin solution. Control over Ru loading was leveraged to produce Ru—MoSelectrocatalysts that demonstrate different nitrogen reduction reaction activities, and which show varying resistance to electrochemical sintering and deactivation. Further, these high surface area materials can be utilized for many applications, including electrocatalysts, supercapacitors, and batteries.


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