The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 20, 2022

Filed:

Apr. 10, 2019
Applicant:

University of Houston System, Houston, TX (US);

Inventors:

Zhifeng Ren, Pearland, TX (US);

Fang Yu, Houston, TX (US);

Haiqing Zhou, Houston, TX (US);

Shuo Chen, Houston, TX (US);

Assignee:

UNIVERSITY OF HOUSTON SYSTEM, Houston, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C23C 16/30 (2006.01); C25B 11/075 (2021.01); C25B 11/061 (2021.01); C25B 1/04 (2021.01); C23C 16/04 (2006.01); C23C 16/18 (2006.01);
U.S. Cl.
CPC ...
C25B 11/075 (2021.01); C23C 16/045 (2013.01); C23C 16/18 (2013.01); C23C 16/30 (2013.01); C25B 1/04 (2013.01); C25B 11/061 (2021.01);
Abstract

A method of manufacturing a bifunctional electrocatalyst for overall water splitting comprising oxygen evolution reaction (OER) and hydrogen evolution reaction (HER) by growing electrocatalyst comprising primarily metallic phosphides on a three-dimensional substrate by: immersing the substrate in an iron nitrate solution to form a once disposed substrate; subjecting the once disposed substrate to thermal phosphidation with phosphorus powder under inert gas to grow metal phosphides thereupon and form a once subjected substrate; cooling the once subjected substrate to form a cooled, once subjected substrate; immersing the cooled, once subjected substrate in an iron nitrate solution to form a twice disposed substrate; and subjecting the twice disposed substrate to thermal phosphidation with phosphorus powder under inert gas to provide an electrode comprising the bifunctional electrocatalyst on the three-dimensional substrate.


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