The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 13, 2022

Filed:

Apr. 07, 2020
Applicant:

The United States of America As Represented BY the Secretary of the Navy, Indian Head, MD (US);

Inventors:

Farhad Forohar, LaPlata, MD (US);

Victor Bellitto, Alexandria, VA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 19/08 (2006.01); C07C 247/14 (2006.01); C25B 15/02 (2021.01); C25B 3/00 (2021.01); C25B 11/057 (2021.01);
U.S. Cl.
CPC ...
C07C 247/14 (2013.01); B01J 19/088 (2013.01); C25B 3/00 (2013.01); C25B 11/057 (2021.01); C25B 15/02 (2013.01); B01J 2219/0809 (2013.01); B01J 2219/0839 (2013.01); B01J 2219/0841 (2013.01); B01J 2219/0877 (2013.01);
Abstract

A method of substituting an azide for hydrogen bonded to a tertiary carbon atom is provided. A liquid mixture in an oxygen-free environment has spaced-apart carbon and platinum electrodes disposed therein. The liquid mixture includes a solvent, ammonium azide, and a base material having at least one tertiary carbon atom with hydrogen bonded thereto. An electric current is applied to the electrodes where the liquid mixture undergoes a reaction. The electrochemically-induced reaction yields a liquid product and a solid product. The liquid product includes the solvent and a constituent having at least one tertiary carbon atom with an azide bonded thereto.


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