The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 16, 2022

Filed:

Jan. 22, 2020
Applicant:

King Fahd University of Petroleum and Minerals, Dhahran, SA;

Inventors:

Salaheldin Elkatatny, Dhahran, SA;

Abdelmjeed Mohamed, Dhahran, SA;

Salem Basfer, Dhahran, SA;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
E21B 37/00 (2006.01); C09K 8/528 (2006.01); E21B 21/00 (2006.01);
U.S. Cl.
CPC ...
C09K 8/528 (2013.01); E21B 37/00 (2013.01); E21B 21/003 (2013.01);
Abstract

A method of removing calcium carbonate-containing oil-based filter cake from a wellbore involving contacting the calcium carbonate-containing oil-based filter cake with a biodegradable acid solution of water, hydrochloric acid, formic acid, citric acid, a surfactant, and a glycol ether mutual solvent. The method is performed at a pressure of 200 to 400 psi and a temperature of 50 to 125° C. The method removes calcium carbonate-containing oil-based filter cake made of a water-in-oil emulsion, calcium carbonate, a primary emulsifier, a secondary emulsifier, a contamination treatment agent, a viscosity control agent, a filtration control agent. The method meets industry standard steel corrosion rates of less than 0.049 lb/ftper day. Also disclosed is a biodegradable acid solution of water, hydrochloric acid, formic acid, citric acid, a surfactant, and a glycol ether mutual solvent that meets OECD 301B thresholds for ready biodegradability.


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