The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 09, 2022

Filed:

Apr. 19, 2017
Applicant:

Inv Nylon Chemicals Americas, Llc, Wilmington, DE (US);

Inventor:

Vinay Medhekar, Beaumont, TX (US);

Assignee:

INV Nylon Chemicals Americas, LLC, Wilmington, DE (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 23/755 (2006.01); B01J 25/02 (2006.01); B01J 35/00 (2006.01); B01J 35/02 (2006.01); B01J 35/10 (2006.01); B01J 37/08 (2006.01); B01J 37/14 (2006.01); B01J 37/18 (2006.01);
U.S. Cl.
CPC ...
B01J 23/755 (2013.01); B01J 25/02 (2013.01); B01J 35/006 (2013.01); B01J 35/0053 (2013.01); B01J 35/023 (2013.01); B01J 35/1009 (2013.01); B01J 35/1014 (2013.01); B01J 35/1019 (2013.01); B01J 37/088 (2013.01); B01J 37/14 (2013.01); B01J 37/18 (2013.01);
Abstract

The present invention relates to heterogeneous catalysts and methods of making and using the same. In various embodiments, the present invention provides a method of making a hydrogenation catalyst including particulate nickel metal (Ni(0)). The method includes calcining first nickel(II)-containing particles in an atmosphere including oxidizing constituents to generate second nickel(II)-containing particles. The method also includes reducing the second nickel(II)-containing particles in a reducing atmosphere while rotating or turning the second nickel(II)-containing particles at about 275° C. to about 360° C. for a time sufficient to generate the particulate nickel metal (Ni(0)), wherein the particulate nickel metal (Ni(0)) is free flowing.


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