The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 12, 2022

Filed:

May. 19, 2017
Applicant:

Shell Oil Company, Houston, TX (US);

Inventors:

Kai Jürgen Fischer, Amsterdam, NL;

Carmelo Perez Golf, Amsterdam, NL;

Pieter Huizenga, Amsterdam, NL;

Assignee:

SHELL USA, INC., Houston, TX (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/84 (2006.01); C07C 29/80 (2006.01);
U.S. Cl.
CPC ...
C07C 29/84 (2013.01); C07C 29/80 (2013.01);
Abstract

The invention provides a process for the separation of a first C3 to C7 diol from a first mixture of C3 to C7 diols. The first mixture is provided to a first distillation column. An extractant is fed to the first distillation column above the first mixture. A stream comprising the first diol and the extractant is removed as a bottoms stream from the first distillation column and subjected to distillation in a second distillation column. A high purity first diol stream is removed from the top section of the second distillation column, while a used extractant stream is removed from the bottom section. The extractant is a C3 to C6 sugar alcohol or mixture thereof. The first diol is a close-boiler to and/or forms an azeotrope with one or more of the other C3 to C7 diols present in the first mixture.


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