The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 31, 2022

Filed:

Aug. 15, 2019
Applicant:

Battelle Memorial Institute, Columbus, OH (US);

Inventors:

Rick Peterson, Columbus, OH (US);

Michael Heinrichs, Columbus, OH (US);

Vinay V. Gadkari, Columbus, OH (US);

Rachid Taha, Dublin, OH (US);

Slawomir Winecki, Dublin, OH (US);

Darwin Argumedo, Columbus, OH (US);

Assignee:

Battelle Memorial Institute, Columbus, OH (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C22B 59/00 (2006.01); C22B 3/06 (2006.01); C22B 3/04 (2006.01); C22B 7/00 (2006.01); C01B 39/02 (2006.01); C22B 3/02 (2006.01); C22B 7/02 (2006.01); C22B 1/00 (2006.01); C01B 39/46 (2006.01); C01B 39/48 (2006.01); C22B 3/12 (2006.01); C22B 21/00 (2006.01);
U.S. Cl.
CPC ...
C22B 59/00 (2013.01); C01B 39/02 (2013.01); C01B 39/46 (2013.01); C01B 39/48 (2013.01); C22B 1/005 (2013.01); C22B 3/02 (2013.01); C22B 3/065 (2013.01); C22B 3/12 (2013.01); C22B 7/007 (2013.01); C22B 7/008 (2013.01); C22B 7/02 (2013.01); C22B 21/0023 (2013.01); Y02P 10/20 (2015.11);
Abstract

A system for recovering rare earth elements from coal ash includes a leaching reactor, an ash dryer downstream of the leaching reactor, and a roaster downstream of the ash dryer that is cooperatively connected to both the leaching reactor and the ash dryer. Coal ash is mixed with an acid stream such that rare earth elements present in the coal ash are dissolved in the acid stream, thereby creating (i) a leachate containing the rare earth elements and (ii) leached ash. The leachate is heated to obtain acid vapor and an acid-soluble rare earth concentrate. Mixing of the coal ash with the acid stream can occur in a leaching reactor and heating of the leachate can occur in a roaster. The acid-soluble rare earth concentrate can be fed to a hydrometallurgical process to separate and purify the rare earth elements.


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