The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 26, 2022

Filed:

Oct. 17, 2019
Applicant:

U.s. Government As Represented BY the Secretary of the Army, Dover, NJ (US);

Inventors:

Neha Mehta, Succasunna, NJ (US);

Jon G. Bragg, Centerbrook, CT (US);

Matthew L. Jorgensen, Centerbrook, CT (US);

Andrew G. Pearsall, Centerbrook, CT (US);

Jerry S. Salan, Centerbrook, CT (US);

Daniel W. Ward, Centerbrook, CT (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07F 1/08 (2006.01); B01J 19/24 (2006.01); C06B 41/00 (2006.01);
U.S. Cl.
CPC ...
C07F 1/08 (2013.01); B01J 19/242 (2013.01); C06B 41/00 (2013.01); B01J 2219/00033 (2013.01); B01J 2219/00081 (2013.01);
Abstract

The present invention is directed to a process for continuous production of copper (I) nitrotetrazolate (DBX-1) by reacting aqueous copper salt with aqueous 5-nitrotetrazolate salt in the presence of a reducing agent. All the reactants are introduced into a continuous flow reactor system, which is composed of a temperature controlled tubular reactor and a mixer that allows for radial mixing. An optional stirred tank reactor may also be incorporated into the process to complete the reaction and allow for crystal growth.


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