The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 12, 2022

Filed:

Dec. 21, 2012
Applicant:

Purac Biochem Bv, Gorinchem, NL;

Inventors:

André Banier De Haan, Best, NL;

Jan Van Krieken, Gorinchem, NL;

Tanja Ðekic {hacek over (Z)}ivkovic, 's-Hertogenbosch, NL;

Assignee:

PURAC BIOCHEM B.V., Gorinchem, NL;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/48 (2006.01); C12P 7/56 (2006.01); B01D 11/04 (2006.01); C07C 51/41 (2006.01);
U.S. Cl.
CPC ...
C07C 51/48 (2013.01); B01D 11/04 (2013.01); C07C 51/412 (2013.01); C12P 7/56 (2013.01); B01D 11/0426 (2013.01);
Abstract

A method for manufacturing carboxylic acid that includes the following steps is provided. First, subjecting an aqueous mixture, including carboxylic acid and at least 5 wt. % dissolved magnesium chloride, to a forward extraction step using a first organic liquid, including an organic solvent, the organic solvent being selected from the group of C5+ ketones, thereby obtaining an organic carboxylic acid solution and an aqueous waste liquid including magnesium chloride. Second, subjecting the organic carboxylic acid solution to a back extraction step wherein the carboxylic acid is extracted from the organic carboxylic acid solution into an aqueous liquid, thereby obtaining an aqueous carboxylic acid solution and a second organic liquid. Third, subjecting the aqueous waste liquid including magnesium chloride derived from the forward extraction to a thermal decomposition step at a temperature of at least 300° C., thereby decomposing the magnesium chloride to magnesium oxide and HCl.


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