The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 05, 2022

Filed:

Mar. 19, 2019
Applicant:

Dh Technologies Development Pte. Ltd., Singapore, SG;

Inventor:

Takashi Baba, Richmond Hill, CA;

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
G16B 40/10 (2019.01); G16C 20/20 (2019.01); G01N 33/68 (2006.01); H01J 49/00 (2006.01);
U.S. Cl.
CPC ...
G16B 40/10 (2019.02); G01N 33/6848 (2013.01); G16C 20/20 (2019.02); H01J 49/005 (2013.01); H01J 49/0036 (2013.01); H01J 49/0054 (2013.01); H01J 49/0068 (2013.01);
Abstract

A mass isolation device selects a precursor ion of a sample that has been digested using a protease. A first fragmentation device fragments the precursor ion using collision-induced dissociation (CID), and the resulting product ions are analyzed using a mass analyzer producing a CID spectrum. A list of theoretical candidate glycopeptide sequences is determined from CID spectrum. The mass isolation device again selects the precursor ion of the sample. A second fragmentation device fragments the precursor ion using electron-based dissociation (ExD), and the resulting product ions are analyzed using the mass analyzer producing a CID spectrum. For each sequence of the list, the sequence is computationally fragmented, producing theoretical fragments, mass-to-charge ratio (m/z) values are calculated for the theoretical fragments, and the sequence is scored using c and z fragment matching rules. The highest scoring sequence is identified as a peptide sequence of a glycopeptide of the sample.


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