The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 22, 2022

Filed:

Aug. 15, 2019
Applicant:

Battelle Memorial Institute, Columbus, OH (US);

Inventors:

Rick Peterson, Columbus, OH (US);

Michael Heinrichs, Columbus, OH (US);

Vinay V. Gadkari, Columbus, OH (US);

Rachid Taha, Dublin, OH (US);

Slawomir Winecki, Dublin, OH (US);

Darwin Argumedo, Columbus, OH (US);

Assignee:

Battelle Memorial Institute, Columbus, OH (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C22B 59/00 (2006.01); C22B 3/06 (2006.01); C22B 7/00 (2006.01); C01B 39/02 (2006.01); C22B 3/02 (2006.01); C22B 7/02 (2006.01); C22B 1/00 (2006.01); C01B 39/46 (2006.01); C01B 39/48 (2006.01); C22B 3/12 (2006.01); C22B 21/00 (2006.01);
U.S. Cl.
CPC ...
C22B 59/00 (2013.01); C01B 39/02 (2013.01); C01B 39/46 (2013.01); C01B 39/48 (2013.01); C22B 1/005 (2013.01); C22B 3/02 (2013.01); C22B 3/065 (2013.01); C22B 3/12 (2013.01); C22B 7/007 (2013.01); C22B 7/008 (2013.01); C22B 7/02 (2013.01); C22B 21/0023 (2013.01); Y02P 10/20 (2015.11);
Abstract

Methods of recovering rare earth elements, vanadium, cobalt, or lithium from coal are described. The coal is dissolved in a first solvent to dissolve organic material in the coal and create a slurry containing coal ash enriched with rare earth elements, vanadium, cobalt, or lithium. The enriched coal ash is separated from the first solvent. Residual organic material is removed from the coal ash. The rare earth elements, vanadium, cobalt, or lithium can then be recovered from the coal ash. The coal ash is mixed with an acid stream that dissolves the rare earth elements, thereby creating (i) a leachate containing the rare earth elements and (ii) leached ash. The leachate is heated to obtain acid vapor and an acid-soluble rare earth concentrate. The acid-soluble rare earth concentrate can be fed to a hydrometallurgical process to separate and purify the rare earth elements.


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