The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 22, 2022

Filed:

Apr. 10, 2019
Applicant:

Nippon Kayaku Kabushiki Kaisha, Tokyo, JP;

Inventors:

Ryota Hiraoka, Yamaguchi, JP;

Shogo Yasuda, Yamaguchi, JP;

Tomoyuki Kawamura, Yamaguchi, JP;

Takanori Nakano, Yamaguchi, JP;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 45/35 (2006.01); C07C 51/00 (2006.01); B01J 23/00 (2006.01); B01J 23/887 (2006.01); C07C 51/235 (2006.01); C07C 47/22 (2006.01);
U.S. Cl.
CPC ...
C07C 45/35 (2013.01); B01J 23/887 (2013.01); C07C 51/235 (2013.01); C07C 47/22 (2013.01);
Abstract

Provided is a method for producing at least one of an unsaturated aldehyde and an unsaturated carboxylic acid from an alkene by an oxidation reaction, in which a n-layered catalyst layer (n≥2) is provided in a gas flow direction in a reaction tube, two or more kinds of catalysts having different activities are used; and the catalysts are packed in such a manner that dT≤20° C. is satisfied, when a difference between a temperature PTof an exothermic peak in a n-th layer as counted from a gas inlet and a minimum value mTof a temperature of a catalyst layer which appears between an exothermic peak in a (n-1)th layer and an exothermic peak in a n-th layer from the gas inlet is represented as dT (=PT−mT), and the change rate of dT is 2.5 or less at a reaction bath temperature within a range of ±6° C. of a reaction bath temperature at which the highest yield is obtained.


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