The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 15, 2022

Filed:

Apr. 19, 2019
Applicant:

Wisconsin Alumni Research Foundation, Madison, WI (US);

Inventors:

Siddarth H. Krishna, Madison, WI (US);

George W. Huber, Middleton, WI (US);

James A. Dumesic, Verona, WI (US);

Assignee:
Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/17 (2006.01); C07C 29/132 (2006.01); C07C 31/24 (2006.01); B01J 21/12 (2006.01); B01J 23/42 (2006.01); B01J 23/44 (2006.01); B01J 23/46 (2006.01);
U.S. Cl.
CPC ...
C07C 29/175 (2013.01); B01J 21/12 (2013.01); B01J 23/42 (2013.01); B01J 23/44 (2013.01); B01J 23/462 (2013.01); B01J 23/464 (2013.01); C07C 29/132 (2013.01); C07C 29/172 (2013.01);
Abstract

A method of making of 1,2,5,6-hexanetetrol ('tetrol'). The method includes the steps of contacting a reaction solution containing water as well as levoglucosenone, dihydrolevoglucosenone, and/or levoglucosanol, with a catalyst containing metal and acid functionalities, at temperature of from about 100° C. to about 175° C., and a hydrogen partial pressure of from about 1 bar to about 50 bar (about 0.1 MPa to about 5 MPa), and for a time wherein at least a portion of the reactant is converted into 1,2,5,6-hexanetetrol.


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