The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 08, 2022

Filed:

Aug. 23, 2019
Applicant:

California Institute of Technology, Pasadena, CA (US);

Inventors:

Katherine T. Faber, Pasadena, CA (US);

Julia A. Kornfield, Pasadena, CA (US);

Noriaki Arai, Pasadena, CA (US);

Orland Bateman, Pasadena, CA (US);

Rustem F. Ismagilov, Pasadena, CA (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C04B 38/06 (2006.01); B01D 67/00 (2006.01); B01D 69/02 (2006.01); B01D 71/02 (2006.01); B01J 35/04 (2006.01); B01J 35/10 (2006.01); C04B 38/00 (2006.01); H01B 1/14 (2006.01); H01B 1/16 (2006.01);
U.S. Cl.
CPC ...
C04B 38/0605 (2013.01); B01D 67/0051 (2013.01); B01D 69/02 (2013.01); B01D 71/024 (2013.01); B01J 35/04 (2013.01); B01J 35/1071 (2013.01); B01J 35/1076 (2013.01); C04B 38/007 (2013.01); C04B 38/0038 (2013.01); C04B 38/0054 (2013.01); C04B 38/0093 (2013.01); H01B 1/14 (2013.01); H01B 1/16 (2013.01); B01D 2325/021 (2013.01); B01D 2325/26 (2013.01);
Abstract

Provided herein are methods for making a freeze-cast material having a internal structure, the methods comprising steps of: determining the internal structure of the material, the internal structure having a plurality of pores, wherein: each of the plurality of pores has directionality; and the step of determining comprises: selecting a temperature gradient and a freezing front velocity to obtain the determined internal structure based on the selected temperature gradient and the selected freezing front velocity; directionally freezing a liquid formulation to form a frozen solid, the step of directionally freezing comprising: controlling the temperature gradient and the freezing front velocity to match the selected temperature gradient and the selected freezing front velocity during directionally freezing; wherein the liquid formulation comprises at least one solvent and at least one dispersed species; and subliming the at least one solvent out of the frozen solid to form the material.


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