The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 08, 2022

Filed:

Jun. 01, 2018
Applicant:

Imam Abdulrahman Bin Faisal University, Dammam, SA;

Inventors:

Ayhan Bozkurt, Dammam, SA;

Seyda Tugba Gunday Anil, Dammam, SA;

Munirah Abdullah Almessiere, Dammam, SA;

Sultan Akhtar, Dammam, SA;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 33/12 (2006.01); C01B 33/18 (2006.01);
U.S. Cl.
CPC ...
C01B 33/18 (2013.01); C01B 33/124 (2013.01); C01P 2004/34 (2013.01); C01P 2004/88 (2013.01); C01P 2006/12 (2013.01); C01P 2006/14 (2013.01); C01P 2006/16 (2013.01);
Abstract

A method for forming hollow silica spheres by dissolving a hydrolyzable aryl silane in an aqueous solution of water and an acid to form a hydrolyzed silane solution, mixing the hydrolyzed silane solution with a hydroxide base to form a precipitate, and calcining the precipitate in a multi-stage calcination procedure that includes (a) heating to a first temperature of 180 to 240° C. with a first ramp rate of 3 to 10° C./min and holding the first temperature for 2 minutes to 2 hours, then (b) heating to a second temperature of 600 to 740° C. at a second ramp rate of 0.1 to 4° C./min, and holding the second temperature for 2 to 24 hours.


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