The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 01, 2022

Filed:

Jan. 08, 2019
Applicant:

Exxonmobil Chemical Patents Inc., Baytown, TX (US);

Inventors:

Constantinos P. Bokis, The Woodlands, TX (US);

Javier Guzman, Porter, TX (US);

Monica D. Lotz, Houston, TX (US);

Michael P. Lanci, Flemington, NJ (US);

Catherine M. Dorsi, Houston, TX (US);

Scott J. Weigel, Allentown, PA (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 7/00 (2006.01); B01D 3/10 (2006.01); C07C 2/66 (2006.01); C07C 2/74 (2006.01); C07C 5/10 (2006.01); C07C 5/27 (2006.01); C07C 5/367 (2006.01); C07C 7/04 (2006.01); C07C 7/14 (2006.01); C07C 15/14 (2006.01);
U.S. Cl.
CPC ...
C07C 7/005 (2013.01); B01D 3/10 (2013.01); C07C 2/66 (2013.01); C07C 2/74 (2013.01); C07C 5/10 (2013.01); C07C 5/2729 (2013.01); C07C 5/367 (2013.01); C07C 7/04 (2013.01); C07C 7/14 (2013.01); C07C 15/14 (2013.01);
Abstract

Processes are described for separating 3,4'- and 4,4′-dimethylbiphenyl from a mixture comprising at least 3,3′-, 3,4′- and 4,4′-dimethylbiphenyl. In the processes, the mixture is cooled to produce a crystallization product comprising at least of the 4,4′-dimethylbiphenyl from the feed mixture and a first mother liquor product. The first mother liquor product is distilled to produce a bottoms stream enriched in 4,4′-dimethylbiphenyl as compared with the first mother liquor product and an overhead stream deficient in 4,4′-dimethylbiphenyl as compared with the first mother liquor product. The overhead stream is then cooled to produce a second crystallization product comprising at least part of the 3,4′-dimethylbiphenyl from the overhead stream and a second mother liquor product.


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