The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 04, 2022

Filed:

Nov. 15, 2019
Applicant:

Jiahua Science & Technology Development (Shanghai) Ltd., Shanghai, CN;

Inventors:

Yandan Chen, Shanghai, CN;

Ke Lai, Shanghai, CN;

Yubo Li, Shanghai, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C08F 220/04 (2006.01); C08F 220/06 (2006.01); C08F 222/04 (2006.01); C08F 222/06 (2006.01); C08F 216/04 (2006.01); C08F 216/08 (2006.01); C08F 216/12 (2006.01); C08F 226/02 (2006.01); C08F 226/04 (2006.01); C08J 3/12 (2006.01); C04B 24/26 (2006.01); C08F 20/06 (2006.01); C08F 22/06 (2006.01); C04B 103/32 (2006.01); C08F 222/02 (2006.01); C08F 216/14 (2006.01);
U.S. Cl.
CPC ...
C08J 3/12 (2013.01); C04B 24/267 (2013.01); C08F 20/06 (2013.01); C08F 22/06 (2013.01); C04B 2103/32 (2013.01); C08F 216/04 (2013.01); C08F 216/08 (2013.01); C08F 216/12 (2013.01); C08F 216/1433 (2020.02); C08F 220/04 (2013.01); C08F 220/06 (2013.01); C08F 222/02 (2013.01); C08F 222/06 (2013.01); C08F 226/02 (2013.01); C08F 226/04 (2013.01); C08J 2333/02 (2013.01); C08J 2337/00 (2013.01);
Abstract

A preparation method of a powdery polycarboxylate superplasticizer is provided, including: mixing a superplasticizer monomer with water to produce a mixture, heating and melting the mixture to produce a melt system; carrying out a bulk polymerization reaction by adding an initiator, a chain transfer agent and an unsaturated carboxylic acid into the melt system, forming a polycarboxylate superplasticizer precursor; and neutralizing and pulverizing the polycarboxylate superplasticizer precursor to produce a powdery polycarboxylate superplasticizer. Water is added in the bulk polymerization and reacts with the superplasticizer monomer and the unsaturated carboxylic acid. While the bulk polymerization reaction is guaranteed to be efficiently carried out and the solid polycarboxylate superplasticizer is formed, the viscosity of a bulk polymerization reaction system is reduced. The superplasticizer is suitable for dry-mixed mortar, high-efficiency concrete and other products.


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