The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Dec. 28, 2021

Filed:

Feb. 20, 2018
Applicant:

Basf SE, Ludwigshafen am Rhein, DE;

Inventors:

Somnath Shivaji Kadam, Ludwigshafen, DE;

Frank Jaekel, Ludwigshafen, DE;

Feelly Ruether, Ludwigshafen, DE;

Lothar Karrer, Ludwigshafen, DE;

Assignee:

BASF SE, Ludwigshafen am Rhein, DE;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C11D 7/32 (2006.01); C11D 7/02 (2006.01); C07C 227/42 (2006.01); B01D 9/00 (2006.01); C07C 229/16 (2006.01); C11D 3/33 (2006.01); C11D 3/39 (2006.01);
U.S. Cl.
CPC ...
C07C 227/42 (2013.01); B01D 9/0036 (2013.01); C07C 229/16 (2013.01); C11D 3/33 (2013.01); C11D 3/39 (2013.01); C11D 7/02 (2013.01); C11D 7/3245 (2013.01); B01D 2009/0086 (2013.01);
Abstract

Process for making solid methylglycine diacetate (MGDA) alkali metal salt (a), said process comprising the steps of (A) providing a 35 to 60% by weight aqueous solution of said MGDA salt having a temperature in the range of from 50 to 90° C., (B) adding 0.01 to 2% by weight of a particulate solid with a pore volume in the range of from 0.25 to 0.75 cm/g, determined by nitrogen adsorption in accordance with 66134:1998-02 (b), the percentage referring to the content of (a), (C) crystallizing (a), (D) removing said crystalline (a) from the mother liquor.


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