The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 30, 2021

Filed:

Nov. 30, 2017
Applicant:

Jiangsu Aosaikang Pharmaceutical Co., Ltd., Jiangsu, CN;

Inventors:

Xiangfeng Chen, Nanjing, CN;

Hongyu Chen, Nanjing, CN;

Shuaihua Tian, Nanjing, CN;

Min Sun, Nanjing, CN;

Changjun Fan, Nanjing, CN;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01N 30/06 (2006.01); C07D 403/06 (2006.01); G01N 30/02 (2006.01);
U.S. Cl.
CPC ...
G01N 30/06 (2013.01); C07D 403/06 (2013.01); G01N 2030/027 (2013.01);
Abstract

A high performance liquid chromatography method used for dexrazoxane-related substances is provided, and in the method, a low-density bonding reversed-phase C18 chromatographic column resistant to pure water is employed; a gradient elution is carried out with mobile phase A and mobile phase B as eluents, the mobile phase A being a buffer, and the mobile phase B being an organic solvent; the volume percent of mobile phase A in eluents in a first stage of the gradient elution is not lower than 90%, and the duration of the first stage of the gradient elution ranges from 15˜30 minutes. By means of the analytical method, dexrazoxane is effectively separated from main impurities, and the qualities of the active pharmaceutical ingredients of dexrazoxane and the preparations thereof could be better controlled.


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