The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 23, 2021

Filed:

Jul. 02, 2019
Applicant:

Industrias Negromex, S.a. DE C.v., Altamira, MX;

Inventors:

Christopher J. Hardiman, Farmington, CT (US);

Xuan Fu, Sugar Land, TX (US);

Robert J. Scribner, Hermann, MO (US);

Julian Maldonado Valenzuela, Tampico, MX;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C08J 3/22 (2006.01); C08K 9/06 (2006.01); B01D 3/38 (2006.01); C08F 6/10 (2006.01); C08J 3/16 (2006.01); C08F 2/44 (2006.01); C08L 21/00 (2006.01); C08L 21/02 (2006.01); C08K 9/00 (2006.01); C08K 9/04 (2006.01);
U.S. Cl.
CPC ...
C08K 9/06 (2013.01); C08F 2/44 (2013.01); C08L 21/00 (2013.01); C08L 21/02 (2013.01); B01D 3/38 (2013.01); C08F 6/10 (2013.01); C08J 3/16 (2013.01); C08J 3/22 (2013.01); C08K 9/00 (2013.01); C08K 9/04 (2013.01); C08L 2310/00 (2013.01); C08L 2314/00 (2013.01);
Abstract

The present invention provides a process for making a silica masterbatch that contains hydrophobated silica, solution-made rubber and emulsion-made rubber. Hydrophobated silica is mixed into a latex emulsion. Solution-rubber crumb in an aqueous suspension is mixed into the latex emulsion, which is coagulated, and a crumb is recovered, further homogenized, dried and baled to yield the silica masterbatch. A well-dispersed mixture of hydrophobated silica and emulsion-made rubber is added into a steam distillation step of a solution-rubber process from which a silica masterbatch is recovered. The emulsion-made rubber can be omitted to make a silica masterbatch of solution rubber and silica without emulsion rubber. The silica masterbatch has physical properties similar to those found in a comparable dry-mixed composition, but the silica masterbatch can be incorporated more easily and less expensively into tires and other rubber products than the dry-mixed composition.


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