The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 12, 2021

Filed:

Jan. 25, 2019
Applicants:

Ifp Energies Nouvelles, Rueil-Malmaison, FR;

Compagnie Generale Des Etablissements Michelin, Clermont-Ferrand, FR;

Inventors:

Frederic Augier, Rueil-Malmaison, FR;

Damien Leinekugel Le Cocq, Rueil-Malmaison, FR;

Rejane Dastillung, Rueil-Malmaison, FR;

Pierre Balz, Rueil-Malmaison, FR;

Assignees:

IFP Energies nouvelles, Rueil-Malmaison, FR;

COMPAGNIE GENERALE DES ETABLISSEMENTS MICHELIN, Clermont-Ferrand, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 29/84 (2006.01); C07C 45/83 (2006.01); B01D 3/14 (2006.01); B01D 11/04 (2006.01); C07C 31/08 (2006.01); C07C 47/06 (2006.01);
U.S. Cl.
CPC ...
B01D 3/14 (2013.01); B01D 11/0426 (2013.01); B01D 11/0488 (2013.01); C07C 29/84 (2013.01); C07C 45/83 (2013.01); C07C 31/08 (2013.01); C07C 47/06 (2013.01);
Abstract

Liquid-liquid extraction and distillation of a liquid feedstock of at least ethanol, water, acetaldehyde and at least one hydrocarbon-based impurity with a boiling point of between 20° C. and 100° C. at atmospheric pressure, or which generates, with at least one of the compounds of the liquid feedstock and/or with the organic extraction solvent and/or with the aqueous back-washing solvent, an azeotrope and a partition coefficient of between 0.1 and 5 at any point in a back-washing (BW) column of the extraction section, by (a) a liquid-liquid extraction step a washing (W) column, a back-washing (BW) column and at least one injection (F) of a cut withdrawn in step b), located in the top half of the back-washing column, (b) distillation of an aldehyde and ethanol separation producing at least one aldehyde-rich effluent, one ethanol-rich effluent and one water-rich effluent.


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