The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 14, 2021

Filed:

Jun. 11, 2018
Applicant:

Jiangsu Nata Opto-electronic Materials Co. Ltd., Jiangsu, CN;

Inventor:

Xiaobing Zhou, Midland, MI (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01B 33/027 (2006.01); C23C 16/40 (2006.01); C01B 33/04 (2006.01); C23C 16/34 (2006.01); C23C 16/455 (2006.01); C01B 6/24 (2006.01); C09D 1/00 (2006.01); C23C 16/50 (2006.01);
U.S. Cl.
CPC ...
C01B 33/046 (2013.01); C01B 6/243 (2013.01); C01B 33/027 (2013.01); C01B 33/04 (2013.01); C09D 1/00 (2013.01); C23C 16/345 (2013.01); C23C 16/401 (2013.01); C23C 16/45536 (2013.01); C23C 16/45553 (2013.01); C23C 16/50 (2013.01);
Abstract

A method of making neopentasilane, the method comprising: contacting perchloroneopentasilane with a reductive effective amount of an alkali metal aluminum hydride in an alkylaluminum compound of formula RAlCl, where R is alkyl having from at least 5 carbon atoms, x is an integer from 1 to 3, and the alkylaluminum compound has a boiling point of at least 250° C., at conditions sufficient to reduce the perchloroneopentasilane, to form a reaction product mixture comprising neopentasilane, and separating the neopentasilane from the product mixture to form a neopentasilane isolate.


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