The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 10, 2021

Filed:

Feb. 09, 2017
Applicants:

Sumitomo Chemical Company, Limited, Tokyo, JP;

Kaken Pharmaceutical Co., Ltd., Tokyo, JP;

Inventors:

Masahiro Takeda, Osaka, JP;

Yohei Tanaka, Osaka, JP;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 207/12 (2006.01); B01J 23/42 (2006.01); B01J 23/44 (2006.01);
U.S. Cl.
CPC ...
C07D 207/12 (2013.01); B01J 23/42 (2013.01); B01J 23/44 (2013.01);
Abstract

The invention relates to a method of producing compound (I) by (A) reacting compound (II) formaldehyde and hydrogen in the presence of a metal catalyst, in a solvent, wherein the amount of the formaldehyde to be used is exceeding 1 mol and not exceeding 5 mol per 1 mol of compound (II), to obtain a mixture containing the formaldehyde and compound (I), and (B) mixing the obtained mixture containing the formaldehyde and compound (I) with hydrogen and a secondary amine selected from the group consisting of diethylamine, dipropylamine, diisopropylamine, butylethylamine, pyrrolidine, piperidine and morpholine, in the presence of a metal catalyst, in a solvent, and then removing the metal catalyst, followed by obtaining the compound (I) by distillation.


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