The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jul. 06, 2021

Filed:

Apr. 03, 2020
Applicant:

Johnson Matthey Davy Technologies Limited, London, GB;

Inventors:

Dena Roberts, Durham, GB;

David John Watson, London, GB;

John Swinney, London, GB;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/12 (2006.01); C07C 67/08 (2006.01); C07C 67/54 (2006.01); C07C 51/09 (2006.01); C07C 59/06 (2006.01); C07C 69/675 (2006.01);
U.S. Cl.
CPC ...
C07C 51/12 (2013.01); C07C 51/09 (2013.01); C07C 59/06 (2013.01); C07C 67/08 (2013.01); C07C 67/54 (2013.01); C07C 69/675 (2013.01); Y02P 20/10 (2015.11);
Abstract

A process for the production of glycolic acid or a derivative thereof comprises: reacting formaldehyde with carbon monoxide and water in a carbonylation reactor in the presence of a sulfur catalyst, said reactor operating under suitable conditions, such that glycolic acid is formed; recovering a first product stream comprising glycolic acid, impurities and a sulfur species in the carbonylation reactor; passing the first product stream to an esterification reactor where it is subjected to esterification to form an alkylglycolate and wherein the esterification is catalysed by the sulfur species recovered in the first product stream; recovering a second product stream comprising the alkylglycolate, sulfur species and impurities from the esterification reactor; separating the sulfur species from the second product stream and recycling it to the carbonylation reactor in step (a) to form a sulphur depleted second product stream; separating the alkylglycolate from the sulphur depleted second product stream in a distillation zone; and recovering the alkylglycolate and converting the alkylglycolate to glycolic acid.


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