The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 29, 2021

Filed:

Sep. 05, 2017
Applicant:

The Administrators of the Tulane Educational Fund, New Orleans, LA (US);

Inventors:

Vijay John, Destrehan, LA (US);

Gary McPherson, Mandeville, LA (US);

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
A61K 9/50 (2006.01); C09B 61/00 (2006.01); C09B 67/08 (2006.01); C09B 11/24 (2006.01); B82Y 30/00 (2011.01); B01J 21/06 (2006.01); B01J 35/00 (2006.01); C09C 1/40 (2006.01); C09C 1/24 (2006.01); C09C 1/30 (2006.01); C09C 1/36 (2006.01); B01J 13/22 (2006.01); B01J 23/745 (2006.01); B01J 13/14 (2006.01); C09B 67/02 (2006.01); A61K 9/51 (2006.01); B01J 21/18 (2006.01); H01M 4/36 (2006.01); H01M 4/587 (2010.01); H01M 4/86 (2006.01); B01J 35/02 (2006.01); B01J 35/10 (2006.01); B01J 37/00 (2006.01); B01J 37/08 (2006.01); H01M 4/90 (2006.01); H01M 10/0525 (2010.01); H01M 10/052 (2010.01); H01G 9/20 (2006.01); B82Y 40/00 (2011.01);
U.S. Cl.
CPC ...
A61K 9/5089 (2013.01); A61K 9/501 (2013.01); A61K 9/5094 (2013.01); A61K 9/51 (2013.01); A61K 9/5192 (2013.01); B01J 13/14 (2013.01); B01J 13/22 (2013.01); B01J 21/063 (2013.01); B01J 21/18 (2013.01); B01J 23/745 (2013.01); B01J 35/002 (2013.01); B01J 35/004 (2013.01); B01J 35/0013 (2013.01); B01J 35/0033 (2013.01); B01J 35/023 (2013.01); B01J 35/026 (2013.01); B01J 35/1057 (2013.01); B01J 35/1061 (2013.01); B01J 35/1066 (2013.01); B01J 37/0072 (2013.01); B01J 37/08 (2013.01); B82Y 30/00 (2013.01); C09B 11/24 (2013.01); C09B 61/00 (2013.01); C09B 67/0008 (2013.01); C09B 67/0097 (2013.01); C09C 1/24 (2013.01); C09C 1/30 (2013.01); C09C 1/3607 (2013.01); C09C 1/407 (2013.01); H01M 4/366 (2013.01); H01M 4/587 (2013.01); H01M 4/8605 (2013.01); H01M 4/8657 (2013.01); H01M 4/9041 (2013.01); H01M 10/0525 (2013.01); B82Y 40/00 (2013.01); C01P 2002/72 (2013.01); C01P 2004/03 (2013.01); C01P 2004/04 (2013.01); C01P 2004/34 (2013.01); C01P 2004/62 (2013.01); C01P 2004/64 (2013.01); C01P 2006/12 (2013.01); C01P 2006/14 (2013.01); C01P 2006/16 (2013.01); C01P 2006/62 (2013.01); H01G 9/2031 (2013.01); H01M 10/052 (2013.01);
Abstract

The present invention discloses the morphology of hollow, double-shelled submicrometer particles generated through a rapid aerosol-based process. The inner shell is an essentially hydrophobic carbon layer of nanoscale dimension (5-20 nm), and the outer shell is a hydrophilic silica layer of approximately 5-40 nm, with the shell thickness being a function of the particle size. The particles are synthesized by exploiting concepts of salt bridging to lock in a surfactant (CTAB) and carbon precursors together with iron species in the interior of a droplet. This deliberate negation of surfactant templating allows a silica shell to form extremely rapidly, sealing in the organic species in the particle interior. Subsequent pyrolysis results in a buildup of internal pressure, forcing carbonaceous species against the silica wall to form an inner shell of carbon. The incorporation of magnetic iron oxide into the shells opens up applications in external stimuli-responsive nanomaterials.


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