The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 22, 2021

Filed:

Oct. 13, 2016
Applicants:

Commissariat a L'energie Atomique ET Aux Energies Alternatives, Paris, FR;

Centre National DE LA Recherche Scientifique (Cnrs), Paris, FR;

Universite DE Picardie Jules Vernes, Amiens, FR;

Inventors:

Nikita Hall, Grenoble, FR;

Sylvain Boulineau, Amiens, FR;

Laurence Croguennec, Saint Selve, FR;

Sébastien Launois, Grenoble, FR;

Christian Masquelier, Boves, FR;

Loïc Simonin, Vinay, FR;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C01B 25/455 (2006.01); H01M 4/58 (2010.01); H01M 10/054 (2010.01); H01M 4/02 (2006.01);
U.S. Cl.
CPC ...
C01B 25/455 (2013.01); H01M 4/5825 (2013.01); C01P 2002/20 (2013.01); C01P 2004/61 (2013.01); C01P 2004/62 (2013.01); C01P 2006/12 (2013.01); C01P 2006/40 (2013.01); H01M 10/054 (2013.01); H01M 2004/028 (2013.01);
Abstract

A method for preparing a NaV(PO)Fmaterial, including at least the steps: a) reducing the vanadium oxide, VO, under a reducing atmosphere in the absence of elementary carbon and in the presence of at least one phosphate anion precursor in order to form vanadium phosphate, VPO; and b) exposing, under an inert atmosphere, a mixture of the VPOmaterial obtained in step a) with an effective amount of sodium fluoride, NaF, and at least one hydrocarbon- and oxygen-containing compound which is a source of elementary carbon, to temperature conditions that are favourable for calcining said mixture so as to form said NaV(PO)Fcompound. Also, a related electrode material, an electrode and a secondary sodium battery using the presented material.


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