The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 08, 2021

Filed:

Mar. 09, 2020
Applicant:

Uchicago Argonne, Llc, Chicago, IL (US);

Inventors:

Trevor L. Dzwiniel, Carol Stream, IL (US);

Krzysztof Pupek, Plainfield, IL (US);

Assignee:

UCHICAGO ARGONNE, LLC, Argonne, IL (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 69/96 (2006.01); C07D 317/40 (2006.01); B01J 31/02 (2006.01);
U.S. Cl.
CPC ...
C07D 317/40 (2013.01); B01J 31/0232 (2013.01); C07C 69/96 (2013.01);
Abstract

In one embodiment, a continuous process for preparing organic carbonate solvent of Formula (I) as described herein comprises contacting a first reactant (an alcohol) with a reactive carbonyl source (carbonyldiimidazole (CDI) or an alkylchloroformate) in the presence of a catalyst in reaction stream flowing through a continuous flow reactor at temperature 20° C. to about 160° C. and at a flow rate providing a residence time in the range of about 0.1 minute to about 24 hours; collecting a reactor effluent exiting from the continuous flow reactor; recovering a crude product from the reactor effluent; and distilling the crude product to obtain the organic carbonate compound of Formula (I). In another embodiment, the first reactant is an epoxide and the carbonyl source is carbon dioxide.


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