The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Patent No.:

US 11027259 B1

PDF
Full Text
Expired
Date of Patent:
Jun. 08, 2021

Filed:

Jan. 20, 2020
Applicant:

Huizhou University, Huizhou, CN;

Inventors:

Jinyun Liao, Huizhou, CN;

Dongsheng Lu, Huizhou, CN;

Hao Li, Huizhou, CN;

Dingshu Xiao, Huizhou, CN;

Assignee:

HUIZHOU UNIVERSITY, Huizhou, CN;

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
B01J 23/00 (2006.01); B01J 23/885 (2006.01); B01J 35/08 (2006.01); B01J 37/00 (2006.01); B01J 37/04 (2006.01); B01J 37/06 (2006.01); B01J 37/08 (2006.01); C01B 3/06 (2006.01); C01G 39/00 (2006.01); C01G 53/00 (2006.01);
U.S. Cl.
CPC ...
B01J 23/885 (2013.01); B01J 35/08 (2013.01); B01J 37/009 (2013.01); B01J 37/04 (2013.01); B01J 37/06 (2013.01); B01J 37/08 (2013.01); C01B 3/06 (2013.01); C01G 39/006 (2013.01); C01G 53/40 (2013.01); C01P 2002/72 (2013.01); C01P 2004/03 (2013.01); C01P 2004/04 (2013.01); C01P 2004/34 (2013.01); C01P 2006/12 (2013.01);
Abstract

A method of preparing hollow molybdate composite microspheres includes steps of: (1) dissolving 1-4 mmol of MClin 20 ml of water to obtain a solution A and dissolving 1-4 mmol. of molybdic acid in 20 ml of water to obtain a solution B, followed by mixing the solution A and the solution B, in which M is Co, Ni, or Cu; (2) dissolving 10-40 mmol of urea in 40 ml of water, adding the mixed solution of step (1) and stirring uniformly; (3) placing the mixed solution of step (2) into a reaction vessel and reacting at 120-160° C. for 6-12 hours; (4) suction filtrating and water washing, followed by drying in a vacuum oven at 40-60° C.; (5) calcination at 350-500° C. for 2-4 hours in a Muffle furnace.


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