The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 25, 2021

Filed:

Mar. 16, 2017
Applicant:

Kri, Inc., Kyoto, JP;

Inventors:

Lianzhen Lin, Kyoto, JP;

Ayako Maruta, Kyoto, JP;

Masanori Hori, Kyoto, JP;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
D21C 3/20 (2006.01); D01F 2/00 (2006.01); C08B 3/20 (2006.01); D21H 11/18 (2006.01); C08B 3/16 (2006.01); D21C 3/00 (2006.01); D21C 3/04 (2006.01); D21C 9/00 (2006.01); D21H 11/20 (2006.01); C08B 3/02 (2006.01); C08B 1/02 (2006.01);
U.S. Cl.
CPC ...
D21C 3/20 (2013.01); C08B 1/02 (2013.01); C08B 3/02 (2013.01); C08B 3/16 (2013.01); C08B 3/20 (2013.01); D01F 2/00 (2013.01); D21C 3/003 (2013.01); D21C 3/04 (2013.01); D21C 9/005 (2013.01); D21H 11/18 (2013.01); D21H 11/20 (2013.01);
Abstract

Provided is a method of producing fine cellulose fibers that are nanosized, that have a high crystallinity degree, and that are less vulnerable to fiber shape damage, the method including impregnating cellulose with a fibrillation solution to fibrillate the cellulose without mechanical crushing, and modifying the cellulose. The method of producing cellulose microfibrils of the present invention includes impregnating cellulose with a fibrillation solution containing a carboxylic acid vinyl ester or an aldehyde and an aprotic solvent having a donor number of 26 or more to fibrillate the cellulose. The aldehyde is at least one kind of aldehyde selected from the group consisting of an aldehyde represented by the following formula (1), paraformaldehyde, cinnamaldehyde, perillaldehyde, vanillin, and glyoxal:R—CHO  (1)where Rrepresents a hydrogen atom, an alkyl group having 1 to 16 carbon atoms, an alkenyl group, a cycloalkyl group, or an aryl group.


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