The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 18, 2021

Filed:

Mar. 14, 2017
Applicant:

Dow Global Technologies Llc, Midland, MI (US);

Inventors:

Junqiang Liu, Manvel, TX (US);

Douglas E. Beyer, Midland, MI (US);

Janet M. Goss, Saginaw, MI (US);

Chan Han, Midland, MI (US);

Edward M. Calverley, Midland, MI (US);

Assignee:

Dow Global Technologies LLC, Midland, MI (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01D 69/02 (2006.01); B01D 53/22 (2006.01); B01D 67/00 (2006.01); B01D 71/02 (2006.01); B01D 71/80 (2006.01); B01D 71/30 (2006.01); B01D 69/08 (2006.01); B01D 71/42 (2006.01); B01D 71/40 (2006.01);
U.S. Cl.
CPC ...
B01D 69/02 (2013.01); B01D 53/228 (2013.01); B01D 67/0067 (2013.01); B01D 71/021 (2013.01); B01D 71/028 (2013.01); B01D 71/30 (2013.01); B01D 71/80 (2013.01); B01D 67/002 (2013.01); B01D 69/08 (2013.01); B01D 71/40 (2013.01); B01D 71/42 (2013.01); B01D 2256/10 (2013.01); B01D 2256/20 (2013.01); B01D 2256/22 (2013.01); B01D 2256/245 (2013.01); B01D 2257/108 (2013.01); B01D 2325/022 (2013.01); B01D 2325/04 (2013.01); B01D 2325/20 (2013.01);
Abstract

A process for separating hydrogen from a gas mixture having hydrogen and a larger gas molecule is comprised of flowing the gas mixture through a carbonized polyvinylidene chloride (PVDC) copolymer membrane having a hydrogen permeance in combination with a hydrogen/methane selectivity, wherein the combination of hydrogen permeance and hydrogen/methane selectivity is (i) at least 30 GPU hydrogen permeance and at least 200 hydrogen/methane selectivity or (ii) at least 10 GPU hydrogen permeance and at least 700 hydrogen/methane selectivity. The carbonized PVDC copolymer may be made by heating and restraining a polyvinylidene chloride copolymer film or hollow fiber having a thickness of 1 micrometer to 250 micrometers to a pretreatment temperature of 100° C. to 180° C. to form a pretreated polyvinylidene chloride copolymer film and then heating and restraining the pretreated polyvinylidene chloride copolymer film to a maximum pyrolysis temperature from 350° C. to 750° C.


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