The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
May. 04, 2021

Filed:

Dec. 20, 2017
Applicant:

Johnson Matthey Davy Technologies Limited, London, GB;

Inventors:

Robert Gallen, London, GB;

Michael William Marshall Tuck, London, GB;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 51/44 (2006.01); B01D 3/14 (2006.01); B01D 3/34 (2006.01); C07C 45/82 (2006.01); C07C 47/04 (2006.01); C07C 57/04 (2006.01);
U.S. Cl.
CPC ...
C07C 51/44 (2013.01); B01D 3/143 (2013.01); B01D 3/34 (2013.01); C07C 45/82 (2013.01); C07C 47/04 (2013.01); C07C 57/04 (2013.01);
Abstract

A process for purification of a crude product stream recovered from the production of an unsaturated carboxylic acid by an aldolization reaction is disclosed. The product stream comprises the unsaturated carboxylic acid, aldehyde, saturated carboxylic acid, water, non-condensable vapours and optionally heavy by-products. The process comprises: providing the crude product stream in the vapour phase to a first separation column operated at a temperature and pressure to form an intermediate product stream comprising product unsaturated carboxylic acid, a portion of the water from the feed stream, a portion of the saturated carboxylic acid and heavy by-products where present; and passing the intermediate product stream to a second separation column operated at a temperature and pressure such that the unsaturated carboxylic acid product is separated and recovered.


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