The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 27, 2021

Filed:

Aug. 11, 2016
Applicant:

Ineos Us Chemicals Company, Naperville, IL (US);

Inventor:

Philip Nubel, Naperville, IL (US);

Assignee:

Ineos US Chemicals Company, Naperville, IL (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B01J 29/04 (2006.01); B01J 29/40 (2006.01); B01J 35/10 (2006.01); C01B 39/02 (2006.01); B01J 29/48 (2006.01); B01J 29/42 (2006.01); C07C 5/27 (2006.01); B01J 35/02 (2006.01); B01J 37/08 (2006.01); C07C 5/22 (2006.01); C07C 15/08 (2006.01);
U.S. Cl.
CPC ...
B01J 29/405 (2013.01); B01J 29/40 (2013.01); B01J 29/42 (2013.01); B01J 29/48 (2013.01); B01J 35/023 (2013.01); B01J 35/109 (2013.01); B01J 35/1014 (2013.01); B01J 35/1019 (2013.01); B01J 35/1057 (2013.01); B01J 35/1061 (2013.01); B01J 37/08 (2013.01); C01B 39/026 (2013.01); C07C 5/222 (2013.01); C07C 5/2737 (2013.01); C07C 5/2775 (2013.01); C07C 15/08 (2013.01); B01J 29/041 (2013.01); B01J 29/042 (2013.01); B01J 29/045 (2013.01); B01J 35/108 (2013.01); B01J 2229/10 (2013.01); B01J 2229/16 (2013.01); B01J 2229/20 (2013.01); B01J 2229/37 (2013.01); B01J 2229/38 (2013.01); B01J 2229/40 (2013.01); C07C 2529/40 (2013.01); C07C 2529/48 (2013.01); Y02P 20/52 (2015.11);
Abstract

A method of making a xylene isomerization catalyst comprises the steps of (i) contacting a ZSM-5 zeolite starting material having a silica to alumina molar ratio of 20 to 50 and having a mesopore surface area in the range of 50 m/gram to 200 m/gram in a reactor with a base to provide an intermediate zeolite material; (ii) recovering the intermediate ZSM-5 zeolite material of step (i); (iii) contacting the intermediate zeolite material with an acid to provide an acid treated ZSM-5 zeolite product; (iv) recovering the acid treated ZSM-5 zeolite material; and (v) calcining the acid treated ZSM-5 zeolite material to provide a desilicated ZSM-5 zeolite product having a silica to alumina molar ratio of 20 to 150 and having a mesopore surface area in the range of 100 m/gram to 400 m/gram.


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