The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 20, 2021

Filed:

Mar. 26, 2020
Applicant:

China University of Geosciences, Wuhan, Hubei, CN;

Inventors:

Zhaochu Hu, Hubei, CN;

Tao He, Hubei, CN;

Wen Zhang, Hubei, CN;

Haihong Chen, Hubei, CN;

Ming Li, Hubei, CN;

Yongsheng Liu, Hubei, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
H01J 49/00 (2006.01); H01J 49/10 (2006.01); G01N 33/24 (2006.01); H01J 49/04 (2006.01); H01J 49/26 (2006.01);
U.S. Cl.
CPC ...
H01J 49/105 (2013.01); G01N 33/24 (2013.01); H01J 49/0459 (2013.01); H01J 49/0468 (2013.01); H01J 49/26 (2013.01);
Abstract

The present invention provides an analysis method for determining halogens in geological samples by ICP-MS. The method includes following steps: weighing a geological sample and ammonium bifluoride in a sample dissolving tank, tightening the sample dissolving tank, and shaking; then heating the sample dissolving tank in a drying oven, and setting a temperature of the drying oven as 200-220° C. and heating time as 1-2 hours; cooling the sample dissolving tank to room temperature so as to obtain a solid mixture after heating is ended, adding ammonium hydroxide into the solid mixture, centrifuging, removing a precipitate, and collecting the supernatant; adding an internal standard solution into the supernatant, and uniformly mixing; and optimizing the ICP-MS to an optimal state, testing content of chlorine in the supernatant under a condition of medium resolution m/Δm=4000, and testing content of bromine and iodine in the supernatant under a condition of low resolution m/Δm=300.


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