The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Apr. 20, 2021

Filed:

May. 17, 2018
Applicant:

Arkema France, Colombes, FR;

Inventors:

Julien Jouanneau, Corneville-sur-Risle, FR;

Jérôme Amstutz, Charly, FR;

Guillaume Vincent, Caen, FR;

Assignee:

ARKEMA FRANCE, Colombes, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 45/51 (2006.01); C07C 45/79 (2006.01); C08G 61/12 (2006.01); C07C 45/81 (2006.01); C07C 45/46 (2006.01); C08L 65/00 (2006.01); C08G 65/40 (2006.01); C07C 45/30 (2006.01);
U.S. Cl.
CPC ...
C07C 45/51 (2013.01); C07C 45/30 (2013.01); C07C 45/46 (2013.01); C07C 45/79 (2013.01); C07C 45/81 (2013.01); C08G 61/127 (2013.01); C08G 65/4012 (2013.01); C08L 65/00 (2013.01); C08G 2261/3442 (2013.01); C08G 2261/45 (2013.01);
Abstract

A method for manufacturing 1,4-bis(4-phenoxybenzoyl)benzene, including: reacting terephthaloyl chloride with diphenyl ether in a reaction solvent and in the presence of a Lewis acid, so as to obtain a product mixture including a 1,4-bis(4-phenoxybenzoyl)benzene-Lewis acid complex; contacting the product mixture with a protic solvent, so as to obtain a first phase containing the Lewis acid and a second phase containing 1,4-bis(4-phenoxybenzoyl)benzene; heating at least the second phase up to a maximum temperature, followed by cooling the second phase down to a separation temperature; subjecting at least the second phase to a solid/liquid separation step at the separation temperature, so as to recover solid 1,4-bis(4-phenoxybenzoyl)benzene.


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