The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 02, 2021

Filed:

Jan. 03, 2019
Applicant:

Government of the United States, As Represented BY the Secretary of the Air Force, Wright-Patterson AFB, OH (US);

Inventors:

James M. Mann, Springboro, OH (US);

Thomas A. Bowen, Beavercreek, OH (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C30B 7/10 (2006.01); C30B 33/02 (2006.01); C30B 29/46 (2006.01); C23C 16/30 (2006.01);
U.S. Cl.
CPC ...
C30B 7/10 (2013.01); C23C 16/305 (2013.01); C30B 29/46 (2013.01); C30B 33/02 (2013.01);
Abstract

Disclosed is a method for synthesizing single crystalline molybdenum disulfide via a hydrothermal process that minimizes or eliminates carbon byproducts. The method involves providing two components, including a source of molybdenum and a mineralizer solution, to an inert reaction vessel, heating one zone sufficiently to dissolve the source of molybdenum in the mineralizer solution, and heating a second zone to a lower temperature to allow thermal transport to drive the dissolved material to the second zone, and then precipitate MoS2 on a seed crystal.


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