The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Mar. 02, 2021

Filed:

Oct. 17, 2017
Applicant:

Battelle Memorial Institute, Richland, WA (US);

Inventors:

John G. Frye, Richland, WA (US);

Kenneth Scott Weil, Richland, WA (US);

Curt A. Lavender, Richland, WA (US);

Jin Yong Kim, Richland, WA (US);

Assignee:

Battelle Memorial Institute, Richland, WA (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
B22F 9/24 (2006.01); C22C 27/00 (2006.01); C22B 34/24 (2006.01); B22F 1/00 (2006.01); C01G 33/00 (2006.01); C01G 41/02 (2006.01); C01G 47/00 (2006.01); C22C 1/04 (2006.01); C22C 1/05 (2006.01); C22C 27/04 (2006.01); C01G 39/02 (2006.01); C22C 27/02 (2006.01); C01B 21/38 (2006.01); C07C 229/06 (2006.01); G01N 23/20 (2018.01);
U.S. Cl.
CPC ...
C22B 34/24 (2013.01); B22F 1/0044 (2013.01); B22F 9/24 (2013.01); C01G 33/00 (2013.01); C01G 39/02 (2013.01); C01G 41/02 (2013.01); C01G 47/00 (2013.01); C22C 1/045 (2013.01); C22C 1/058 (2013.01); C22C 27/00 (2013.01); C22C 27/02 (2013.01); C22C 27/04 (2013.01); B22F 2301/20 (2013.01); C01B 21/38 (2013.01); C07C 229/06 (2013.01); G01N 23/20075 (2013.01);
Abstract

Methods are provided for synthesizing high purity niobium or rhenium powders by a combustion reaction. The methods can include: forming a combustion synthesis solution by dissolving in water an oxidizer, a fuel, and at least one base-soluble, ammonium salt of niobium or rhenium in amounts that yield a stoichiometric burn when combusted; and heating the combustion synthesis solution to a temperature sufficient to substantially remove the water and to initiate a self-sustaining combustion reaction.


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