The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Feb. 02, 2021

Filed:

Dec. 11, 2017
Applicant:

Basf SE, Ludwigshafen am Rhein, DE;

Inventors:

Ortmund Lang, Ludwigshafen, DE;

Bernd Metzen, Ludwigshafen, DE;

Claus Hechler, Ludwigshafen, DE;

Assignee:

BASF SE, Ludwigshafen am Rhein, DE;

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C07C 67/54 (2006.01); B01D 3/14 (2006.01); B01D 3/42 (2006.01); C07C 69/54 (2006.01);
U.S. Cl.
CPC ...
C07C 67/54 (2013.01); B01D 3/141 (2013.01); B01D 3/148 (2013.01); B01D 3/42 (2013.01); C07C 69/54 (2013.01);
Abstract

A process for isolating pure butyl acrylate from crude butyl acrylate, which is carried out in a dividing wall column having separation-active internals and a vaporizer, and in which: a dividing wall is arranged in a longitudinal direction of the column to form an upper joint column region, a lower joint column region, an inflow section having a side feed point and an offtake section having a side offtake point; a ratio of an amount of liquid at an upper end of the dividing wall going to an enrichment section and a stripping section of the column is set in the range from 1:0.2 to 1:5; and a ratio of an amount of vapor streams at a lower end of the dividing wall going to the stripping section and the enrichment section of the column is set in a range from 1:0.5 to 1:2.0.


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