The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 26, 2021

Filed:

Dec. 14, 2016
Applicant:

Arkema France, Colombes, FR;

Inventors:

Abdelatif Baba-Ahmed, Saint-fons, FR;

Bertrand Collier, Saint-genis-laval, FR;

Dominique Deur-Bert, Charly, FR;

Laurent Wendlinger, Soucieu en Jarrest, FR;

Assignee:

Arkema France, Colombes, FR;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 17/386 (2006.01); C07C 17/38 (2006.01); C07C 19/08 (2006.01); C07C 21/18 (2006.01); C07C 17/383 (2006.01); C09K 5/04 (2006.01);
U.S. Cl.
CPC ...
C07C 21/18 (2013.01); C07C 17/383 (2013.01); C07C 17/386 (2013.01); C07C 19/08 (2013.01); C09K 5/045 (2013.01); C09K 2205/126 (2013.01);
Abstract

The invention relates to a method for purifying 1,1,1,2,2-pentafluoropropane (245cb) using a first composition comprising 1,1,1,2,2-pentafluoropropane and at least one of the compounds selected from the group consisting of 1,1-difluoroethane (152a), 1,1,1,2-tetrafluoroethane (134a), trans-1,3,3,3-tetrafluoro-1-propene (1234ze-E), cis-1,3,3,3-tetrafluoro-1-propene (1234ze-Z), trans-1,2,3,3,3-pentafluoropropene (1225ye-E), cis-1,2,3,3,3-10 pentafluoropropene (1225ye-Z) and 3,3,3-trifluoropropene (1243zf), said method comprising the steps of: a) bringing said first composition into contact with at least one organic extraction agent in order to form a second composition; b) extractive distillation of said second composition in order to form i) a third composition comprising said organic extraction agent and said at least one of the compounds selected from the group consisting of 1,1-difluoroethane (152a), 1,1,1,2-tetrafluoroethane (134a), trans-1,3,3,3-tetrafluoro-1-propene (1234ze-E), cis-1,3,3,3-tetrafluoro-1-propene (1234ze-Z), trans-1,2,3,3,3-pentafluoropropene (1225ye-E), cis-1,2,3,3,3-pentafluoropropene (1225ye-Z) and 3,3,3-trifluoropropene (1243zf); and ii) a stream comprising the 1,1,1,2,2-pentafluoropropane; and c) recovery and separation of said third composition. The invention also relates to a method for producing 1234yf including the method for purifying 1,1,2,2-pentafluoropropane.


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