The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jan. 26, 2021

Filed:

Nov. 18, 2016
Applicant:

Rohm and Haas Company, Collegeville, PA (US);

Inventors:

William C. Finch, Ambler, PA (US);

Mike McGinnis, Collegeville, PA (US);

Sudhir M. Mulik, North Wales, PA (US);

Charles J. Rand, Philadelphia, PA (US);

Assignee:

Rohm and Haas Company, Collegeville, PA (US);

Attorney:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
C04B 24/24 (2006.01); C04B 24/26 (2006.01); C08F 120/06 (2006.01); C08F 2/38 (2006.01); C08F 2/02 (2006.01); C08G 81/02 (2006.01); C04B 103/32 (2006.01);
U.S. Cl.
CPC ...
C04B 24/246 (2013.01); C04B 24/2647 (2013.01); C04B 24/2658 (2013.01); C08F 2/02 (2013.01); C08F 2/38 (2013.01); C08F 120/06 (2013.01); C08G 81/02 (2013.01); C04B 2103/32 (2013.01);
Abstract

The present invention provides efficient methods to form a high solids content polymeric polyacid or a comb polymer useful as a superplasticizer or dispersant which comprise heating to from 80 to 100 C. for a first time period, and then, sequentially, heating to a second temperature of from 150 to 250° C. for a second time period a wet reaction mixture having a solids content of from 80 to 99 wt. % and comprising from 15 to 60 wt. % of one or more ethylenically unsaturated acid or a salt thereof, from 37 to 76.99 wt. % of one or more polyether polyols, alkyl polyether polyols, polyether amines or alkyl polyether amines in the presence of (i) from 0.01 to 1 wt. %, of one or more water soluble radical initiators or redox pairs and (ii) from 2 to 22 wt. % of one or more phosphorus oxide containing compounds, all weights based on the total weight of the wet reaction mixture.


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