The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 24, 2020

Filed:

Feb. 08, 2019
Applicant:

SI Group, Inc., Schenectady, NY (US);

Inventors:

Cornelius Haase, Schenectady, NY (US);

Jeff Hiscock, Schenectady, NY (US);

Philip David Atwood, Schenectady, NY (US);

Assignee:

SI GROUP, INC., Schenectady, NY (US);

Attorneys:
Primary Examiner:
Int. Cl.
CPC ...
C07C 37/20 (2006.01); C07C 39/17 (2006.01); C07C 37/52 (2006.01); B01D 9/00 (2006.01); B01J 23/04 (2006.01);
U.S. Cl.
CPC ...
C07C 37/52 (2013.01); C07C 37/20 (2013.01); B01D 9/0054 (2013.01); B01J 23/04 (2013.01); C07C 39/17 (2013.01); C07C 2603/92 (2017.05);
Abstract

This invention relates to a one-pot synthesis of a high-purity calix[4]arene compound by reacting a phenolic compound and an aldehyde in the presence of at least one nitrogen-containing base as a catalyst to form the calix[8]arene compound, and cleaving the calix[8]arene compound into a high-purity calix[4]arene compound, directly, without carrying out a purification step before the cleaving step. The invention also relates to an improved conversion of a calix[8]arene compound to a calix[4]arene compound, by cleaving a calix[8]arene compound in a glycol ether solvent having a boiling point of at least about 200° C., to result in a high-purity calix[4]arene compound, without using an antisolvent.


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