The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Nov. 10, 2020

Filed:

Nov. 13, 2018
Applicant:

Eastman Chemical Company, Kingsport, TN (US);

Inventors:

Sumit Chakraborty, Johnson City, TN (US);

Steven J. Adams, Gray, TN (US);

Robert Thomas Hembre, Johnson City, TN (US);

Scott Donald Barnicki, Kingsport, TN (US);

David Alan Jenkins, Jonesborough, TN (US);

Assignee:

Eastman Chemical Company, Kingsport, TN (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 67/03 (2006.01); B01J 27/232 (2006.01); B01J 31/02 (2006.01); C07C 69/708 (2006.01);
U.S. Cl.
CPC ...
C07C 67/03 (2013.01); B01J 27/232 (2013.01); B01J 31/0212 (2013.01); B01J 2531/46 (2013.01); C07C 69/708 (2013.01);
Abstract

A process for the transesterification of methyl-2-ethylhexanoate with triethylene glycol to produce triethylene glycol di-2-ethylhexanoate is provided. In the process, methyl-2-ethylhexanoate is combined with triethylene glycol to form a first mixture. The first mixture is heated in the presence of a catalyst to form a second mixture comprising methanol and triethylene glycol di-2-ethylhexanoate. Methanol is separated from the second mixture to yield triethylene glycol di-2-ethylhexanoate. NaCO, CsCO, KCO, RbCO, sodium methoxide or titanium isopropoxide are suitable catalysts.


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