The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 27, 2020

Filed:

May. 23, 2017
Applicants:

Institute of Materia Medica, Chinese Academy of Medical Sciences, Beijing, CN;

Tianjin Chase Sun Pharmaceutical Co., Ltd, Tianjin, CN;

Inventors:

Zhiqiang Feng, Beijing, CN;

Xiaoguang Chen, Beijing, CN;

Yang Yang, Beijing, CN;

Fangfang Lai, Beijing, CN;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07D 401/14 (2006.01); C07D 295/155 (2006.01); C07C 233/36 (2006.01); C07C 255/54 (2006.01); C07D 405/12 (2006.01); C07C 311/05 (2006.01); C07D 319/18 (2006.01); C07D 207/16 (2006.01); C07C 45/61 (2006.01); C07C 231/12 (2006.01); A61P 35/00 (2006.01); C07C 211/29 (2006.01); C07C 229/36 (2006.01); C07C 235/34 (2006.01); C07D 221/00 (2006.01); C07D 265/30 (2006.01); C07D 407/12 (2006.01); C07C 227/12 (2006.01); C07C 269/02 (2006.01); C07C 271/64 (2006.01); C07D 207/08 (2006.01); C07D 309/14 (2006.01); C07D 319/16 (2006.01); A61K 31/36 (2006.01); A61K 31/165 (2006.01); A61K 31/277 (2006.01); A61K 45/06 (2006.01);
U.S. Cl.
CPC ...
C07D 295/155 (2013.01); A61P 35/00 (2018.01); C07C 45/61 (2013.01); C07C 211/29 (2013.01); C07C 227/12 (2013.01); C07C 229/36 (2013.01); C07C 231/12 (2013.01); C07C 233/36 (2013.01); C07C 235/34 (2013.01); C07C 255/54 (2013.01); C07C 269/02 (2013.01); C07C 271/64 (2013.01); C07C 311/05 (2013.01); C07D 207/08 (2013.01); C07D 207/16 (2013.01); C07D 221/00 (2013.01); C07D 265/30 (2013.01); C07D 309/14 (2013.01); C07D 319/16 (2013.01); C07D 319/18 (2013.01); C07D 401/14 (2013.01); C07D 405/12 (2013.01); C07D 407/12 (2013.01); A61K 31/165 (2013.01); A61K 31/277 (2013.01); A61K 31/36 (2013.01); A61K 45/06 (2013.01);
Abstract

Provided is a method for preparing 2-hydroxy-4-(2, 3-disubstituted benzyloxy)-5-substituted benzaldehyde derivative represented by formula (I). The method comprises the following steps: (1) preparing 3-aryl-2-substituted toluene derivative 2 by using 3-iodo-2-substituted toluene derivative 1 and aryl boronic acid 5 or aryl boronate as starting materials; (2) preparing a benzyl halide derivative 3 by using 3-aryl-2-substituted toluene derivative 2 as starting materials; and (3) preparing 4-(2, 3-disubstituted benzyloxy)-2-hydroxy-5-substituted benzaldehyde derivative (I) by using benzyl halide derivative 3 and 2,4-dihydroxy-5-substituted benzaldehyde 6.


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