The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 27, 2020

Filed:

Mar. 21, 2016
Applicants:

Toyota Motor Engineering & Manufacturing North America, Inc., Erlanger, KY (US);

The University of Manitoba, Winnipeg, CA;

Inventors:

Elizabeth Marie Skoropata, Winnipeg, CA;

Michael Paul Rowe, Pinckney, MI (US);

Johan Alexander van Lierop, Winnipeg, CA;

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
B22F 9/30 (2006.01); B22F 1/00 (2006.01); C07F 5/02 (2006.01); C07F 19/00 (2006.01); B82Y 40/00 (2011.01); B82Y 30/00 (2011.01);
U.S. Cl.
CPC ...
B22F 9/30 (2013.01); B22F 1/0044 (2013.01); C07F 19/00 (2013.01); B22F 2301/30 (2013.01); B22F 2304/05 (2013.01); B82Y 30/00 (2013.01); B82Y 40/00 (2013.01);
Abstract

A method for synthesizing a reagent complex includes a step of ball-milling a mixture that includes: a powder of a zero-valent element; a hydride molecule; and a nitrile ligand. The method produces a reagent complex having a formula Q.X.L, where Qis the zero-valent element, X is the hydride molecule, and L is the nitrile ligand. A process for synthesizing nanoparticles composed of the zero-valent element includes a step of adding solvent to the reagent complex. Crystal texture of the nanoparticles is modulated by appropriate selection of the molar ratio nitrile ligand in the reagent complex.


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