The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Oct. 13, 2020

Filed:

Jul. 18, 2017
Applicant:

The Government of the United States of America, As Represented BY the Secretary of the Navy, Arlington, VA (US);

Inventors:

Adam L. Friedman, Silver Spring, MD (US);

F. Keith Perkins, Alexandria, VA (US);

James C. Culbertson, Alexandria, VA (US);

Aubrey T. Hanbicki, Washington, DC (US);

Paul M. Campbell, Alexandria, VA (US);

Attorneys:
Primary Examiner:
Assistant Examiner:
Int. Cl.
CPC ...
G01N 27/26 (2006.01); C07C 211/05 (2006.01); C01G 35/00 (2006.01); C01G 39/06 (2006.01); C01G 41/00 (2006.01); C01G 33/00 (2006.01); C07C 211/07 (2006.01); C01B 19/04 (2006.01); G01N 27/12 (2006.01); G01N 21/77 (2006.01); G01N 21/65 (2006.01); G01N 21/78 (2006.01); C12N 9/16 (2006.01); G01N 21/64 (2006.01); H04B 7/00 (2006.01);
U.S. Cl.
CPC ...
G01N 27/26 (2013.01); C01B 19/04 (2013.01); C01G 33/00 (2013.01); C01G 35/00 (2013.01); C01G 39/06 (2013.01); C01G 41/00 (2013.01); C07C 211/05 (2013.01); C07C 211/07 (2013.01); G01N 21/65 (2013.01); G01N 21/77 (2013.01); G01N 27/125 (2013.01); C12N 9/16 (2013.01); G01N 21/64 (2013.01); G01N 21/783 (2013.01); H04B 7/00 (2013.01);
Abstract

Optical and electronic detection of chemicals, and particularly strong electron-donors, by 2H to 1T phase-based transition metal dichalcogenide (TMD) films, detection apparatus incorporating the TMD films, methods for forming the detection apparatus, and detection systems and methods based on the TMD films are provided. The detection apparatus includes a 2H phase TMD film that transitions to the 1T phase under exposure to strong electron donors. After exposure, the phase state can be determined to assess whether all or a portion of the TMD has undergone a transition from the 2H phase to the 1T phase. Following detection, TMD films in the 1T phase can be converted back to the 2H phase, resulting in a reusable chemical sensor that is selective for strong electron donors.


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