The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 29, 2020

Filed:

Sep. 07, 2016
Applicant:

Okinawa Institute of Science and Technology School Corporation, Kunigami-Gun, Okinawa, JP;

Inventors:

Yabing Qi, Kunigami-gun, JP;

Min-cherl Jung, Kunigami-gun, JP;

Sonia Ruiz Raga, Kunigami-gun, JP;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
H01G 9/20 (2006.01); C23C 14/24 (2006.01); H01L 51/42 (2006.01); C23C 14/06 (2006.01); C23C 14/58 (2006.01); H01L 51/00 (2006.01);
U.S. Cl.
CPC ...
H01G 9/2009 (2013.01); C23C 14/0694 (2013.01); C23C 14/24 (2013.01); C23C 14/5806 (2013.01); C23C 14/5893 (2013.01); H01L 51/001 (2013.01); H01L 51/4213 (2013.01); Y02E 10/549 (2013.01); Y02P 70/521 (2015.11);
Abstract

A method of forming a Pb-free perovskite film is provided, the method based on vacuum evaporation and comprising: first depositing a first material comprising Sn halide on a substrate to form a first layer; second depositing a second material comprising organic halide to form a second layer on the first layer to obtain a sequentially-deposited two-layer film on the substrate; and annealing the sequentially-deposited two-layer film on the substrate. During the annealing, the first and second materials inter-diffuse and react to form the Pb-free perovskite film. The second layer is formed to cover the first layer so as to prevent the first layer from air exposure. The solar cell device including the Pb-free perovskite film formed by using the present method exhibits good stability.


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