The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Sep. 22, 2020

Filed:

Oct. 18, 2019
Applicant:

Nan Ya Plastics Corporation, Taipei, TW;

Inventors:

Te-Chao Liao, Taipei, TW;

Jung-Jen Chuang, Taipei, TW;

Chung-Yu Chen, Taipei, TW;

Chia-Ruey Tsai, Taipei, TW;

Sung-Chieh Chao, Taipei, TW;

Assignee:
Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 67/303 (2006.01); B01J 23/46 (2006.01); B01J 21/04 (2006.01); B01J 8/10 (2006.01); B01J 8/08 (2006.01);
U.S. Cl.
CPC ...
C07C 67/303 (2013.01); B01J 8/085 (2013.01); B01J 8/087 (2013.01); B01J 8/10 (2013.01); B01J 21/04 (2013.01); B01J 23/462 (2013.01); B01J 2208/0015 (2013.01); B01J 2208/00141 (2013.01); B01J 2208/00867 (2013.01);
Abstract

A hydrogenation method for increasing the yield of cyclohexane-1,4-dicarboxylic acid diisooctyl ester is provided. The hydrogenation method uses a hydrogenating reaction tank, which is equipped with a hollow-shaft gas-introducing mixer having air-extracting, air-exhausting and mixing functions, to allow hydrogen gas to be uniformly dispersed in a reaction solution. A ruthenium-on-alumina (Ru/AlO) hydrogenation catalyst can be used for carrying out a hydrogenation reaction under gentle conditions. Therefore, the hydrogenation catalyst can be used in a reduced amount, the risk of side reaction(s) can be reduced, and the yield of cyclohexane-1,4-dicarboxylic acid diisooctyl ester can reach at least 99% with a cis isomer proportion of at least 85.0%. The hydrogenation method shows extremely high economic benefit.


Find Patent Forward Citations

Loading…