The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Aug. 18, 2020

Filed:

Jan. 30, 2019
Applicant:

Hunan Jinyuan New Materials Co., Ltd., Yiyang, CN;

Inventors:

Xunbing Liu, Yiyang, CN;

Jianjun Ouyang, Yiyang, CN;

Xijuan Liu, Yiyang, CN;

Assignee:

Other;

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C01D 15/00 (2006.01); C01D 15/08 (2006.01); C22B 26/12 (2006.01); H01M 10/54 (2006.01);
U.S. Cl.
CPC ...
C01D 15/08 (2013.01); C22B 26/12 (2013.01); H01M 10/54 (2013.01);
Abstract

A method for preparing industrial grade lithium carbonate from crude lithium fluoride includes the following steps: a, pulping by stirring crude lithium fluoride into a pulp, and adding an acid to prepare a crude lithium fluoride pulp-like material; b, double decomposition by adding the lithium fluoride pulp-like material obtained in the step a into a boiling calcium chloride solution, and then adding an alkaline substance to obtain a lithium chloride solution; c, lithium carbonate precipitation by heating the lithium chloride solution obtained in the step b, adding a carbonate solution according to the mass of lithium in the lithium chloride solution, stirring at a constant temperature, and filtering, wherein the filter cake is a lithium carbonate product. The lithium fluoride is decomposed at one time in a low-acidity environment; fluoride ions are removed; and a double decomposition reaction is used to decompose the lithium fluoride into lithium ions and calcium fluoride precipitates.


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