The patent badge is an abbreviated version of the USPTO patent document. The patent badge does contain a link to the full patent document.

The patent badge is an abbreviated version of the USPTO patent document. The patent badge covers the following: Patent number, Date patent was issued, Date patent was filed, Title of the patent, Applicant, Inventor, Assignee, Attorney firm, Primary examiner, Assistant examiner, CPCs, and Abstract. The patent badge does contain a link to the full patent document (in Adobe Acrobat format, aka pdf). To download or print any patent click here.

Date of Patent:
Jun. 30, 2020

Filed:

Dec. 10, 2018
Applicant:

Valvoline Licensing and Intellectual Property Llc, Lexington, KY (US);

Inventors:

Rajkumar Rajule, Dist. Thane, IN;

Jesse Dambacher, Lexington, KY (US);

Attorney:
Primary Examiner:
Int. Cl.
CPC ...
C07C 5/10 (2006.01); C07C 7/12 (2006.01); G01N 30/92 (2006.01); B01D 15/10 (2006.01);
U.S. Cl.
CPC ...
C07C 5/10 (2013.01); C07C 7/12 (2013.01); G01N 30/92 (2013.01); B01D 15/10 (2013.01); C07C 2523/46 (2013.01); C07C 2601/14 (2017.05);
Abstract

A procedure for hydrogenation of alpha dimethyl styrene dimer that is scalable, economical, and safe is provided. These processes routinely provide greater than a 98% yield and require no purification step. The methods of producing hydrogenated alpha dimethyl styrene dimer comprising adding to a reactor under nitrogen a catalyst comprising Ru/C or Rh/C and an alpha dimethyl styrene dimer to form a catalyst and alpha dimethyl styrene dimer reaction mixture. The reaction mixture is then heated under pressure until hydrogenation of the alpha dimethyl styrene dimer is complete. To recover the hydrogenated alpha dimethyl styrene dimer, the reaction mixture is filtered through a celite bed under nitrogen.


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